• Advanced Characterisation of Natural and Synthetic Rubbers

Size Exclusion, Gel Permeation Chromatography (GPC)

Advanced Characterisation of Natural and Synthetic Rubbers

Jan 13 2017

At the recent International Symposium on GPC/SEC and Related Techniques in Amsterdam, Postnova Analytics presented a well-received lecture entitled 'Comprehensive Characterization of Natural Rubber Samples using Thermal Field-Flow-Fractionation coupled with MALS and Triple Detection'.

The presentation by Dr Gerhard Heinzmann included an informative introduction to the Thermal Field Flow Fractionation (TF3) technique, a comparison of the technique versus using GPC/SEC and application examples including data from a complex natural rubber sample.

The speaker explained how advantageously TF3 is able to separate samples by both particle size and chemical composition at the same time. Further he showed how unlike traditional GPC/SEC separation, TF3 offers huge flexibility in choice of fractionation power and avoids interactions with stationery phase, degradation due to shear stress and the need for sample filtration. Also beneficially the TF3 technique has no size exclusion limit and therefore even ultra-high molecular weight, branched and cross-linked natural and synthetic rubbers can be separated using the methodology.

In conclusion the lecture showed how thermal field flow fractionation coupled with MALS and triple detection provides a highly efficient method of separating and characterising complex, high molecular weight natural or synthetic rubbers at high resolution in organic and aqueous solvents.

For more information please click here.


Digital Edition

Chromatography Today - Buyers' Guide 2022

October 2023

In This Edition Modern & Practical Applications - Accelerating ADC Development with Mass Spectrometry - Implementing High-Resolution Ion Mobility into Peptide Mapping Workflows Chromatogr...

View all digital editions

Events

analytica 2024

Apr 09 2024 Munich, Germany

Korea Lab 2024

Apr 23 2024 Kintex, South Korea

Korea Chem 2024

Apr 23 2024 Seoul, South Korea

AOCS Annual Meeting & Expo

Apr 28 2024 Montreal, Quebec, Canada

SETAC Europe

May 05 2024 Seville, Spain

View all events